Considerable efforts are being given to develop commercially viable technologies in order to alleviate the dependence on hydrocarbons as well as to reduce carbon dioxide emission by the use of fossil fuel. The proton exchange membrane fuel cell (PEMFC) has emerged as one of the most promising clean energy technology for residential and automotive applications. The high power density, low operating temperature, convenient fuel supply, longer lifetime, and modularity are the attractive features of PEMFC. This book covers the detailed methodology for development and characterization of composite bipolar plate for PEMFC. It also includes the methodology for synthesis and characterization of graphene. The synthesized monolayer graphene was used as one of the reinforcements for the composite bipolar plate. The state of the art for development and performance evaluation of PEMFC is discussed in detail. The information presented in this book will be helpful to the researchers, academicians, and manufacturers for the development of the composite bipolar plate for PEMFC.