This book discusses various electrochemical methods and their validation in chemotherapeutic drugs analysis and their progress and great impact on analytical chemistry. A great number of studies on chemotherapeutic drugs such as zolinza, zanosar and zinecard by various electroanalytical techniques. Electrochemical analysis often offers advantages over other analytical methods, such as a high degree of accuracy, precision, selectivity and also low cost of operation. It also focuses on collection of samples, experimental procedures and environmental and health issues concerning chemical technology are also addressed. The book consists of four chapters discussing various topics with updated references. The author is a highly qualified electroanalytical chemist with an impressive record of publication in the field of electrochemistry and is to be commended for a job well done.